Nickel Chloride Promoted Glaser Coupling Reaction in Hot Water

A Glaser coupling reaction of terminal alkynes in the presence of nickel chloride withoutany organics and bases in hot water has been developed, which produces the correspondinghomo-coupling products in good yields.     

The First and Facile Synthesis of (±) Syringaresinol

The first and facile synthesis of (±)syringaresinol was described.     

Space time-index plots for probing dynamical nonstationarity

We propose a simple method to efficiently probe dynamical nonstationarity in observed time series. In a space time-index plot, the density distributions as a function of normalized time-index are V-shaped due to nonstationarity. We show that this method is workable for short data sets and typical examples are illustrated.     

第I类非自共轭锥上的Gamma函数

本文将Ｇａｍｍａ函数及Ｓｉｅｇｅｌ积分推广到一般的第Ｉ类非自共轭锥上．作为其应用，显式给出了以这些锥为底的管状域（或第一类Ｓｉｅｇｅｌ域）的Ｃａｕｃｈｙ Ｓｚｅｇ¨ｏ核和形式Ｐｏｉｓｏｎ核．     

激光相位成像雷达的研究

利用无合作目标漫反射激光相位测距的原理,对关键单元技术进行分析和设计,研制成一种用于自主式车辆视觉导引的激光相位成像雷达的原理样机.     

保健酒中淫羊霍苷成分的分析研究

采用高效液相色谱法对某保健酒中淫羊藿苷成分进行分析研究,结果表明,保健酒中淫羊藿苷的平均含量为0.627％,平均回收率为98.1％,相对标准差（RSD）为2.1％.本分析方法也适用于其他保健酒、药材和药品中淫羊藿苷成分的分析测定.     

起爆药爆轰场和燃烧场的干涉法显示及其图像处理

本文介绍了利用脉冲YAG激光引爆起爆药产生爆轰流场或燃烧温度场,用时间序列干涉法首次获得了爆轰流场和起始燃烧过程的时间序列干涉图的实验结果.在此基础上,采用条纹曲线检测法和双三次多结点插值样条函数从干涉图上提取爆轰场冲击波的波阵面,并通过序列波阵面配准算法,定量地计算了冲击波的传播速度.同时,还定量计算了燃烧场温度随时间变化的分布.     

FAR-INFRARED AND INFRARED REFLECTIONS OF Tl2Ba2Ca2Cu3O10 FILM

The far-infrared and infrared reflection spectra of Tl₂Ba₂Ca₂Cu₃O₁₀ superconducting film are reported in this paper. It is found there are three sharp reflection edges in both the superconducting and normal states, their positions being near ≈ 150, ≈ 350 and ≈600 cm^-1. We attribute these reflection spectra to the Drude free carriers and a wide mid-infrared absorption band. When the incident angle increases from 7° to 30°, some additional stractures appear in the refiection spectra, which are the A_2u phonon modes vibrating along c-axis.     

η-Invariant and Flat Vector Bundles

Abstract We present an alternate definition of the mod Z component of the Atiyah-Patodi-Singer η invariant associated to (not necessary unitary) flat vector bundles, which identifies explicitly its real and imaginary parts. This is done by combining a deformation of flat connections introduced in a previous paper with the analytic continuation procedure appearing in the original article of Atiyah, Patodi and Singer. * Project supported by the Cheung-Kong Scholarship of the Ministry of Education of China and the 973 Project of the Ministry of Science and Technology of China. (Dedicated to the memory of Shiing-Shen Chern)     

第一讲中子散射与散裂中子源

中子散射是研究物质微观结构和动态的理想工具之一,广泛地应用于凝聚态物质研究和应用的众多学科领域.散裂中子源能是新一代的加速器基脉冲中子源,能为中子散射提供高通量的脉冲中子.文章简明地介绍了中子散射的特点和它作为物质结构和动态探针的优越性,以及散裂中子源的基本原理、发展状况和多学科的应用优势.我国计划建设的散裂中子源CSNS中,靶站将由多片钨靶、铍/铁反射体和铁/重混凝土生物屏蔽体组成.质子束功率100kW下,脉冲中子通量约为2.4×1016n/cm2/s.第一期将设计建造高通量粉末衍射仪、高分辨粉末衍射仪、小角散射仪、多功能反射仪和直接几何非弹性散射仪等五台典型的中子散射谱仪,以覆盖大部分的中子散射研究领域.